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SYNTHESIS AND PHYSICO-CHEMICAL PROPERTIES OF A NEW COMPLEX FERRITE
Дата публикации
1 октября 2024 г.
Тип
journal article
Издатель
National Academy of Sciences of the Republic of Kazakhstan
Выпуск
3
Первая страница
137
Последняя страница
146
ISSN
2224-5286
Аннотация
The article discusses the synthesis of new complex ferrite, radiographic and electron microscopic studies. The phase of complex ferrites was synthesized by the method of high-temperature sol-gel synthesis. For the first time, the structure of CrKFe2O5 Composite ferrite was studied by X-ray phase analysis and scanning electron microscope methods, the syngony type, elementary cell parameters, radiographic and pycnometric densities, and elemental analysis were determined. A comparative analysis of the relationship between the parameters of the Crystal cell of primary substances and the parameters of the obtained complex ferrite Crystal cell was carried out. Micro-samples were taken from different parts of the crystallite obtained through a scanning electron microscope, the elemental composition of the crystals was analyzed, and the general type of layer of the complex ferrite surface was demonstrated. As a result, the fact that the compound consists of two phases, the clarity of its construction was determined by the topography and chemical composition of the compound. As a result, it was found that the newly synthesized complex ferrite corresponds to the Formula CrKFe2O5. The particle size of the compounds formed is large (between 200 μm, 20.0 μm, 5.00 μm and 2.00 μm).
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